2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

Base Information

Chemical Name:2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester
CAS No.:100655-29-6
Molecular Formula:C₂₉H₄₇N₂O₈PSi
Molecular Weight:610.76
Hs Code.:

2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

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Chemical Property of 2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

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Technology Process of 2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

There total 5 articles about 2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 100655-29-6
2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) THF, 0 deg C, 1 h, 2.) THF, 20 deg C, 12 h

2: 1.) NaH / 1.) THF, 20 deg C, 2 h, 2.) THF, 20 deg C, 12 h

3: 83 percent / 30percent aq. H₂O₂ / CH₂Cl₂; H₂O / 1 h / 20 °C

4: CH₂Cl₂ / 12 h / 20 °C

With dihydrogen peroxide; sodium hydride; In dichloromethane; water;
DOI:10.1021/jo00359a029

Reference yield:

: 79414-13-4
trimethylsilylethyl bromoacetate

: 100655-29-6
2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) THF, 0 deg C, 1 h, 2.) THF, 20 deg C, 12 h

2: 1.) NaH / 1.) THF, 20 deg C, 2 h, 2.) THF, 20 deg C, 12 h

3: 83 percent / 30percent aq. H₂O₂ / CH₂Cl₂; H₂O / 1 h / 20 °C

4: CH₂Cl₂ / 12 h / 20 °C

With dihydrogen peroxide; sodium hydride; In dichloromethane; water;
DOI:10.1021/jo00359a029

Reference yield:

: 100604-45-3
1-ethyl 4-<2-(trimethylsilyl)ethyl> 2-(diethoxyphosphinyl)butanedioate

: 100655-29-6
2-(Diethoxy-phosphoryl)-3-[(2S,3S)-2-((E)-1,1-dimethyl-3-phenyl-allyl)-3-methyl-4-oxo-[1,2]diazetidin-1-yl]-succinic acid 1-ethyl ester 4-(2-trimethylsilanyl-ethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 20 deg C, 2 h, 2.) THF, 20 deg C, 12 h

2: 83 percent / 30percent aq. H₂O₂ / CH₂Cl₂; H₂O / 1 h / 20 °C

3: CH₂Cl₂ / 12 h / 20 °C

With dihydrogen peroxide; sodium hydride; In dichloromethane; water;
DOI:10.1021/jo00359a029