N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14

Base Information

• Chemical Name: N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14
• CAS No.: 98453-03-3
• Molecular Formula: C₄₇H₃₃NO₄
• Molecular Weight: 675.783

Synonyms:

Chemical Property of N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14

Chemical Property:

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Technology Process of N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14

There total 3 articles about N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N-methylmaleimide (930-88-1) + rubrene endoperoxyde (32287-37-9) → epoxy-5,12 phenoxy-5 triphenyl-6,11,12 dihydro-5,12 naphtacene (98480-37-6) + 11b-phenoxy-5a,6,11-triphenyl-5a,11b-dihydro-naphto<2,3-3',4'>cyclobuta<1',2',-2,3>benzofuran (98453-02-2) + epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne (38135-74-9) + N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (98453-03-3)

Guidance literature:

In benzene; at 15 ℃; for 27h; Irradiation;

Reference yield: 2.0%

rubrene endoperoxyde (32287-37-9) → epoxy-5,12 phenoxy-5 triphenyl-6,11,12 dihydro-5,12 naphtacene (98480-37-6) + 11b-phenoxy-5a,6,11-triphenyl-5a,11b-dihydro-naphto<2,3-3',4'>cyclobuta<1',2',-2,3>benzofuran (98453-02-2) + epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne (38135-74-9) + N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (98453-03-3)

Guidance literature:

With N-methylmaleimide; In benzene; at 15 ℃; for 27h; Irradiation;

Reference yield:

rubrene endoperoxyde (32287-37-9) → hydroxy-12 triphenyl-6,11,12, oxo-5 dihydro-5,12 naphtacene (98453-01-1) + epoxy-5,12 phenoxy-5 triphenyl-6,11,12 dihydro-5,12 naphtacene (98480-37-6) + 11b-phenoxy-5a,6,11-triphenyl-5a,11b-dihydro-naphto<2,3-3',4'>cyclobuta<1',2',-2,3>benzofuran (98453-02-2) + epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne (38135-74-9) + N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (98453-03-3)

Guidance literature:

In benzene; at 15 ℃; Mechanism; Irradiation; in the presence or absence of N-methylmaleimide;

upstream raw materials:

N-methylmaleimide

rubrene endoperoxyde

Downstream raw materials:

N-methyl ethano-1,4 dihydro-1,4 tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (exo)

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