Re2(μ-O2CCH)4(O2CCH3)2

Base Information

Chemical Name:Re2(μ-O2CCH)4(O2CCH3)2
CAS No.:119391-20-7
Molecular Formula:C₁₂H₁₈O₁₂Re₂
Molecular Weight:726.682
Hs Code.:

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Chemical Property of Re2(μ-O2CCH)4(O2CCH3)2

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Technology Process of Re2(μ-O2CCH)4(O2CCH3)2

There total 1 articles about Re2(μ-O2CCH)4(O2CCH3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 2Re⁽⁴⁺⁾*8H^(1-)*4P(C₆H₅)3=Re₂H₈(P(C₆H₅)3)4

: 119391-20-7
Re2(μ-O2CCH)4(O2CCH3)2

: 59751-32-5
[Re(CO)₂(OAc)(PPh₃)₂]

Guidance literature:: With CH₃COOH; (CH₃CO)2O; In 1,2-dichloro-benzene; (N2); mixt. of acetic acid and acetic anhydride was refluxed with soln. of Re complex for 4 h, filtered from ppt.; pptn. of Re2(O2CCH3)6 was washed with ether; elem. anal.; to filtrate was added ether and slowly evapd.; after refrigerating about 2 weeks crystals of Re(O2CCH3)2(CO)2(PPh3)2 were filtered off, washed with ether and dried in vac.; elem. anal.;

Reference yield: 82.0%

: 119391-20-7
Re2(μ-O2CCH)4(O2CCH3)2

: 33612-87-2,14126-96-6,15628-76-9
dirhenium(III) dichlorotetra-μ-acetate

Guidance literature:: With HCl; In ethanol; (N2); slurry of Re complex was stirred in EtOH at 0°C, HCl gas was bubbled through soln. for 3 min.; formed orange pptn. was filtered off and dried; identified IR and electronic spect.;