hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene

Base Information

Chemical Name:hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene
CAS No.:123835-07-4
Molecular Formula:C₇H₈*C₂₈H₆₄Cl₆P₄Ti₂
Molecular Weight:925.33
Hs Code.:

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Chemical Property of hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene

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Technology Process of hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene

There total 2 articles about hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 31168-87-3,18039-90-2
titanium trichloride tris(tetrahydrofuran)

: 87532-69-2
1,1'-(1,2-ethanediyl)bis[1,1-bis(1-methylethyl)phosphine]

: 123835-07-4
hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene

Guidance literature:: In toluene; under Ar, addn. of P-compound to a suspension of Ti-complex in toluene, soln. turned purple, stirred for 1 h, filtered, concd., cooling to -20°C, pptn.; elem. anal.;

Reference yield: 14.0%

: 31168-87-3,18039-90-2
titanium trichloride tris(tetrahydrofuran)

: 87532-69-2
1,1'-(1,2-ethanediyl)bis[1,1-bis(1-methylethyl)phosphine]

: 123835-08-5
trchloro(tetrahydrofuran){1,2-bis(diisopropylphosphino)ethane}titanium(III)

: 123835-07-4
hexachlorobis{1,2-bis(diisopropylphosphino)ethane}dititanium(III)-toluene

Guidance literature:: In diethyl ether; under Ar, addn. of P-compound to a suspension of Ti-complex in diethyl ether, soln. turned green, pptn. of a purple solid, stirred for 5 h, filtered, concd., cooling to -20°C, pptn.; elem. anal.;