mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

Base Information

Chemical Name:mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)
CAS No.:110096-49-6
Molecular Formula:C₄₁H₃₉Cl₂OP₃Ru
Molecular Weight:812.657
Hs Code.:

mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

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Chemical Property of mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

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Technology Process of mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

There total 2 articles about mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.4%

: 110096-47-4
trans, trans, trans-dichlorodicarbonylbis(vinyldiphenylphosphine)ruthenium(II)

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 110096-49-6
mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diphenylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

Guidance literature:: In dichloromethane; under N2; soln. stirred for ca. 24 h at room temp.; filtration, concn., addn. of ethanol, ppt. washed with ethanol, anhydrous Et2O, vacuum-dried overnight, elem. anal.;
DOI:10.1021/ic00321a019

Reference yield:

: 110096-47-4
trans, trans, trans-dichlorodicarbonylbis(vinyldiphenylphosphine)ruthenium(II)

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 110096-49-6
mer-trans-dichlorocarbonyl(vinyldiphenylphosphine)(2-(diphenylphosphino)-5,6-dimethyl-7-phenylphosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

Guidance literature:: In chloroform; 24 h at room temp. under nitrogen; characterized spectroscopically and by X-ray analysis;
DOI:10.1021/om00153a042