tetraphenylammonium tetrakis(benzenethiolato)nickelate(II)

Base Information

Chemical Name:tetraphenylammonium tetrakis(benzenethiolato)nickelate(II)
CAS No.:57927-74-9
Molecular Formula:2C₂₄H₂₀N*C₂₄H₂₀NiS₄
Molecular Weight:1140.24
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylammonium tetrakis(benzenethiolato)nickelate(II)

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Technology Process of tetraphenylammonium tetrakis(benzenethiolato)nickelate(II)

There total 1 articles about tetraphenylammonium tetrakis(benzenethiolato)nickelate(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: tetraphenylammonium benzenethiolate

: tetraethylammonium tetrachloroniccolate(II)

: 57927-74-9
tetraphenylammonium tetrakis(benzenethiolato)nickelate(II)

Guidance literature:: In acetonitrile; addn. of Ni-complex to soln. of thiolate under N2 with stirring, the colour rapidly turns dark red brown; filtn., recrystn. (70°C, CH3CN), elem. anal.;

Reference yield: 52.0%

: 57927-74-9
2P(C₆H₅)4⁽¹⁺⁾*Ni(S(C₆H₅))4^(2-)=(P(C₆H₅)4)2(Ni(S(C₆H₅))4)

: 6493-73-8
dibenzyltrisulfide

: 93780-88-2
2P(C₆H₅)4⁽¹⁺⁾*Ni(S₄)2^(2-)=(P(C₆H₅)4)2Ni(S₄)2

Guidance literature:: In acetonitrile; to a soln. of Ni-complex in CH3CN was added solid ligand, mixt. was stirred for 5 min, Et2O was added, crystals formed after several h;; collected, washed with Et2O, dried; elem. anal.;;