methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate

Base Information

Chemical Name:methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate
CAS No.:52443-31-9
Molecular Formula:C₄₄H₄₇Cl₃O₂₃
Molecular Weight:1050.2
Hs Code.:

methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate

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Chemical Property of methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate

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Technology Process of methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate

There total 2 articles about methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52443-29-5
C₄₁H₄₁Cl₃O₂₂

: 52443-31-9,78418-60-7
methyl 3,5-di-O-benzoyl-2-O-<2,3,6-tri-O-acetyl-4-O-2,2,2-trichloroethyl(-2,3-di-O-acetyl-β-D-ribofuranosid-5-yl)-α-D-glucopyranosyl>-(2R)-allaro-1,4-lactone-6-ate

Guidance literature:: Multi-step reaction with 2 steps

1: water / pyridine / 100 °C

2: pyridine / 1 h / Ambient temperature

With pyridine; water; In pyridine;
DOI:10.1135/cccc19810667