2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

Base Information

Chemical Name:2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate
CAS No.:1108614-49-8
Molecular Formula:C₃₁H₃₂N₆O₆
Molecular Weight:584.632
Hs Code.:

2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

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Chemical Property of 2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

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Technology Process of 2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

There total 5 articles about 2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-[(E)-2-(4-methoxyphenyl)ethenyl]nicotinoyl chloride

: C₁₆H₂₁N₅O₄

: 1108614-49-8
2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl-formamide;
DOI:10.1039/b814452d

Reference yield:

: 1000277-47-3
6-[(E)-2-(4-methoxyphenyl)ethenyl]nicotinic acid

: 1108614-49-8
2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane / 1 h / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 3 h

With thionyl chloride; palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2012.08.013

Reference yield:

: 1108614-51-2
2-{[(1-methyl-4-nitro-1H-pyrrol-2-yl)carbonyl]amino}ethyl acetate

: 1108614-49-8
2-[({4-[({4-[({6-[(E)-2-(4-methoxyphenyl)ethenyl]-3-pyridinyl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}-carbonyl)amino]-1-methyl-1H-pyrrol-2-yl}carbonyl)amino]ethyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 3 h

2: 4-methyl-morpholine / N,N-dimethyl-formamide

3: palladium 10% on activated carbon; hydrogen / methanol / 3 h

With 4-methyl-morpholine; palladium 10% on activated carbon; hydrogen; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.013