2,3,4-trimethyl-1-nitromethylbenzene

Base Information

• Chemical Name: 2,3,4-trimethyl-1-nitromethylbenzene
• CAS No.: 60367-93-3
• Molecular Formula: C₁₀H₁₃NO₂
• Molecular Weight: 179.219
• Mol file: 60367-93-3.mol

Synonyms:

Chemical Property of 2,3,4-trimethyl-1-nitromethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4-trimethyl-1-nitromethylbenzene

There total 2 articles about 2,3,4-trimethyl-1-nitromethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3,4-Tetramethylbenzene (488-23-3) → 2,3,4,5-tetramethyl-1-nitrobenzene (42887-62-7) + 2,3,4-trimethyl-1-nitromethylbenzene (60367-93-3) + 1,2,3,4-tetramethyl-r-3-nitro-t-6-trinitromethylcyclohexa-1,4-diene + 2,3,4,5-tetramethyl-1-trinitromethylbenzene

Guidance literature:

With tetranitromethane; In acetonitrile; at 20 ℃; for 6h; Further byproducts given;

DOI:10.3891/acta.chem.scand.50-0735

Reference yield:

tetranitromethane (509-14-8) + 1,2,3,4-Tetramethylbenzene (488-23-3) → 2,3,4,5-tetramethyl-1-nitrobenzene (42887-62-7) + 2,3,4-trimethyl-1-nitromethylbenzene (60367-93-3) + 1,2,3,4-tetramethyl-r-3-nitro-t-6-trinitromethylcyclohexa-1,4-diene + 2,3,4,5-tetramethyl-1-trinitromethylbenzene

Guidance literature:

In acetonitrile; at 20 ℃; for 6h; Further byproducts given;

DOI:10.3891/acta.chem.scand.50-0735

Reference yield:

2,3,4-trimethyl-1-nitromethylbenzene (60367-93-3) → 2,3,4-trimethylbenzaldehyde (34341-28-1)

Guidance literature:

With potassium permanganate;

upstream raw materials:

tetranitromethane

1,2,3,4-Tetramethylbenzene

Downstream raw materials:

2,3,4-trimethylbenzaldehyde