C₄₇H₇₄O₁₀Si

Base Information

Chemical Name:C₄₇H₇₄O₁₀Si
CAS No.:954106-31-1
Molecular Formula:C₄₇H₇₄O₁₀Si
Molecular Weight:827.184
Hs Code.:

C<sub>47</sub>H<sub>74</sub>O<sub>10</sub>Si

Synonyms:

Suppliers and Price of C₄₇H₇₄O₁₀Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₇H₇₄O₁₀Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₇H₇₄O₁₀Si

There total 20 articles about C₄₇H₇₄O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 954106-23-1
C₃₇H₄₅NO₆

: 954106-31-1
C₄₇H₇₄O₁₀Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: 92 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

2.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

3.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

4.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

4.2: Me₃SiCl / 0.58 h / -78 - 0 °C

5.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

6.1: n-Bu₂SnO / toluene / 0.75 h / Heating

6.2: 71 percent / CH₂Cl₂ / 1 h / 0 °C

7.1: imidazole / dimethylformamide / 3 h / 65 °C

7.2: dimethylformamide / 20 h / 80 °C

8.1: 0.174 g / DDQ / CH₂Cl₂; H₂O / 1.5 h / 20 °C

9.1: O₃; N-methylmorpholine N-oxide; benzyl ethyl eter / CH₂Cl₂ / 0.13 h / -78 °C

9.2: 80 percent / NaBH₄ / methanol / 1 h / -40 - -10 °C

10.1: DMSO; (COCl)2; Et₃N / CH₂Cl₂ / 1.67 h / -78 - 0 °C

11.1: 0.112 g / Bn₂NH*CF₃COOH / toluene / 16 h / 45 °C

12.1: NaBH₄ / ethanol / 1 h / -78 - 0 °C

12.2: aq. HF; pyridine / tetrahydrofuran / 9 h / 20 °C

12.3: 81 percent / i-Pr₂NEt; tetra-n-butylammonium iodide / CH₂Cl₂ / 10 h / 50 °C

With 1H-imidazole; dmap; lithium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; hydrogen; dihydrogen peroxide; di(n-butyl)tin oxide; potassium carbonate; ozone; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 4.1: Ireland-Claisen rearrngement / 10.1: Swern oxidation reaction;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-39-9
C₂₅H₃₁NO₄

: 954106-31-1
C₄₇H₇₄O₁₀Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: NaHDMS / tetrahydrofuran / 2 h / -78 °C

1.2: 80 percent / tetrahydrofuran / -78 - -20 °C

2.1: 92 percent / LiOH*H₂O; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

3.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

4.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

5.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

5.2: Me₃SiCl / 0.58 h / -78 - 0 °C

6.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

7.1: n-Bu₂SnO / toluene / 0.75 h / Heating

7.2: 71 percent / CH₂Cl₂ / 1 h / 0 °C

8.1: imidazole / dimethylformamide / 3 h / 65 °C

8.2: dimethylformamide / 20 h / 80 °C

9.1: 0.174 g / DDQ / CH₂Cl₂; H₂O / 1.5 h / 20 °C

10.1: O₃; N-methylmorpholine N-oxide; benzyl ethyl eter / CH₂Cl₂ / 0.13 h / -78 °C

10.2: 80 percent / NaBH₄ / methanol / 1 h / -40 - -10 °C

11.1: DMSO; (COCl)2; Et₃N / CH₂Cl₂ / 1.67 h / -78 - 0 °C

12.1: 0.112 g / Bn₂NH*CF₃COOH / toluene / 16 h / 45 °C

13.1: NaBH₄ / ethanol / 1 h / -78 - 0 °C

13.2: aq. HF; pyridine / tetrahydrofuran / 9 h / 20 °C

13.3: 81 percent / i-Pr₂NEt; tetra-n-butylammonium iodide / CH₂Cl₂ / 10 h / 50 °C

With 1H-imidazole; dmap; lithium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; di(n-butyl)tin oxide; potassium carbonate; ozone; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 5.1: Ireland-Claisen rearrngement / 11.1: Swern oxidation reaction;
DOI:10.1016/j.tetlet.2007.07.182

Reference yield:

: 954106-40-2
C₂₇H₃₆O₅

: 954106-31-1
C₄₇H₇₄O₁₀Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 96 percent / H₂; K₂CO₃ / Pd/C / methanol / 0.83 h

2.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C

3.1: ((S)-1-Ph-2-piperidin-1-yl-Et)-(2,2,2-triF-Et)amine; n-BuLi / tetrahydrofuran; hexane / 1 h

3.2: Me₃SiCl / 0.58 h / -78 - 0 °C

4.1: 0.310 g / LiAlH₄ / tetrahydrofuran / 5 h / Heating

5.1: n-Bu₂SnO / toluene / 0.75 h / Heating

5.2: 71 percent / CH₂Cl₂ / 1 h / 0 °C

6.1: imidazole / dimethylformamide / 3 h / 65 °C

6.2: dimethylformamide / 20 h / 80 °C

7.1: 0.174 g / DDQ / CH₂Cl₂; H₂O / 1.5 h / 20 °C

8.1: O₃; N-methylmorpholine N-oxide; benzyl ethyl eter / CH₂Cl₂ / 0.13 h / -78 °C

8.2: 80 percent / NaBH₄ / methanol / 1 h / -40 - -10 °C

9.1: DMSO; (COCl)2; Et₃N / CH₂Cl₂ / 1.67 h / -78 - 0 °C

10.1: 0.112 g / Bn₂NH*CF₃COOH / toluene / 16 h / 45 °C

11.1: NaBH₄ / ethanol / 1 h / -78 - 0 °C

11.2: aq. HF; pyridine / tetrahydrofuran / 9 h / 20 °C

11.3: 81 percent / i-Pr₂NEt; tetra-n-butylammonium iodide / CH₂Cl₂ / 10 h / 50 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; hydrogen; di(n-butyl)tin oxide; potassium carbonate; ozone; dimethyl sulfoxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; 3.1: Ireland-Claisen rearrngement / 9.1: Swern oxidation reaction;
DOI:10.1016/j.tetlet.2007.07.182