Re(P(p-C₆H₄OMe)3)2H₇

Base Information

• Chemical Name: Re(P(p-C₆H₄OMe)3)2H₇
• CAS No.: 108034-79-3
• Molecular Formula: C₄₂H₄₉O₆P₂Re
• Molecular Weight: 898.002

Synonyms:

Chemical Property of Re(P(p-C₆H₄OMe)3)2H₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Re(P(p-C₆H₄OMe)3)2H₇

There total 1 articles about Re(P(p-C₆H₄OMe)3)2H₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

OReCl3(tris(p-methoxyphenyl)phosphine)2 (108009-09-2) → Re(P(p-C6H4OMe)3)2H7 (108034-79-3)

Guidance literature:

With lithium aluminium hydride; In diethyl ether; ReOCl3(P(p-C6H4OMe)3)2 was was placed under vac. for 1 h, ether was vac.transferred into the flask, LiAlH4 was added over 10 min, kept for 30 min; filtered, filtrate was evapd., excess LiAlH4 was decompd. by wet CH2Cl2 (-40°C) and H2O (0°C) under N2, mixt. was filtered, cooled by addn. of liq. N2, decanted, evapd. (10**-3 Torr), residue was washed with Et2O under N2, dried under vac.;

Reference yield:

Re(P(p-C6H4OMe)3)2H7 (108034-79-3) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → CpRe(P(p-C6H4OMe)3)2H2

Guidance literature:

In tetrahydrofuran; THF soln. of the Re-complex was treated with 100 equiv of cyclopentadiene under inert atmosphere followed by gentle heating; elem. anal.;

upstream raw materials:

OReCl₃(tris(p-methoxyphenyl)phosphine)2

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 108034-79-3 Re(P(p-C₆H₄OMe)3)2H₇

Send

Send

Metric Ton KG G Pound L ML

Send

Send