[RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]

Base Information

Chemical Name:[RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]
CAS No.:123932-01-4
Molecular Formula:C₄₂H₄₂Cl₂P₄Ru
Molecular Weight:842.667
Hs Code.:

[RuCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)]

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Chemical Property of [RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]

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Technology Process of [RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]

There total 2 articles about [RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: dichlorotetrakis(dimethylsulfoxide)ruthenium(II)

: 162872-01-7,163879-29-6,23582-04-9,52186-58-0,54294-46-1
[R-(R(*),R(*))]-(-)-1,1,4,7,10,10-hexaphenyl-1,4,7,10-tetraphosphadecane

: 85436-57-3,62660-76-8,123932-01-4
[RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]

: [RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]

Guidance literature:: In toluene; under exclusion of air and moisture, soln. of the org. compound was added dropwise to Ru-compound in refluxing toluene, refluxed for 1.5 h; solvent removed under reduced pressure, washed (hexane);

Reference yield:

: 16997-43-6,30059-47-3,35986-78-8
trans-dichlorotetrakis(pyridine-N)ruthenium(II)

: 23582-04-9,52186-58-0,54294-46-1,162872-01-7,163879-29-6
tetraphos

: 123932-01-4,62660-76-8,85436-57-3
trans-dichloro(hexaphenyl-1,4,7,10-tetraphosphadecane)ruthenium(II)

Guidance literature:: In toluene; Ru(pyr)4Cl2 and equimolar amt. TETRAPHOS 1 refluxed in toluene for 8 h under Ar atm.; soln. evapd. and cooled to -10°C; elem. anal.;
DOI:10.1016/S0020-1693(00)87598-2

Reference yield: 46.0%

: 16853-85-3
lithium aluminium tetrahydride

: 85436-57-3,62660-76-8,123932-01-4
[RuCl₂((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)]

: 157240-17-0,62630-50-6
trans-[hydridochlororuthenium(II)(mesotetraphos)]

Guidance literature:: With ethanol; In tetrahydrofuran; under exclusion of air and moisture, LiAlH4 added to a soln. of Ru-compound under stirring, refluxed for 24 h, cooled, EtOH added, solvent evapd., bezene added, stirred overnight; filtered (Celite), filtrate reduced to dryness, washed (hexane), dried;elem. anal.;