methyl tricyclohexylstannanedithiocarboxylate

Base Information

Chemical Name:methyl tricyclohexylstannanedithiocarboxylate
CAS No.:86927-64-2
Molecular Formula:C₂₀H₃₆S₂Sn
Molecular Weight:459.348
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl tricyclohexylstannanedithiocarboxylate

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Technology Process of methyl tricyclohexylstannanedithiocarboxylate

There total 1 articles about methyl tricyclohexylstannanedithiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 3091-32-5
tricyclohexyltin(IV) chloride

: 86927-64-2
methyl tricyclohexylstannanedithiocarboxylate

Guidance literature:: With carbon disulfide; lithium; methyl iodide; In tetrahydrofuran; byproducts: LiI; redn. of Sn compd. soln. with Li (excess) under N2, 5d; filtration overglass wool; addn. of CS2; addn. of CH3I (slight excess); chromy. (silica gel, THF/petroleum ether); evapn.; washing (ethanol); elem. anal.;

Reference yield: 36.0%

: dicarbonyl(η(5)-cyclopentadienyl)manganese(THF)

: 86927-64-2
methyl tricyclohexylstannanedithiocarboxylate

: 86921-15-5
dicarbonyl(η5-cyclopentadienyl)(methyl tricyclohexylstannanedithiocarboxylate)manganese

Guidance literature:: In tetrahydrofuran; addn. of Mn complex soln. (excess) to ester soln. under N2; reducing volume; chromy. (silica gel, THF/petroleum ether); evapn.; freezing; triturating with methanol; solidification; elem. anal.;