Δ-(-)D-[Co(phen)2(S-Phe)](ClO4)2*2H2O

Base Information

• Chemical Name: Δ-(-)D-[Co(phen)2(S-Phe)](ClO4)2*2H2O
• CAS No.: 81097-87-2
• Molecular Formula: C₃₃H₂₆CoN₅O₂*2ClO₄*2H₂O
• Molecular Weight: 818.527

Synonyms:

Chemical Property of Δ-(-)D-[Co(phen)2(S-Phe)](ClO4)2*2H2O

Chemical Property:

Purity/Quality:

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Technology Process of Δ-(-)D-[Co(phen)2(S-Phe)](ClO4)2*2H2O

There total 1 articles about Δ-(-)D-[Co(phen)2(S-Phe)](ClO4)2*2H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-{Co(1,10-phenanthroline)2Cl2}Cl*3H2O + L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) + sodium perchlorate → Δ-(-)D-[Co(phen)2(S-Phe)](ClO4)2*2H2O (81097-87-2) + Λ-(+)D-[Co(phen)2(S-Phe)](ClO4)2 (81176-57-0)

Guidance literature:

With sodium ethanolate; In methanol; solid complex was added to a soln. of acid and NaOEt, stirred at 40°C for 3 h; chromy. (CM-Sephadex, aq. Na2SO4), NaClO4 was added, cooling, filtration, washing with ethanol-water 1:1, ethanol, recrystn. (water), air drying; elem. anal.;

DOI:10.1021/ic00136a075

upstream raw materials:

L-phenylalanine

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