(η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate

Base Information

Chemical Name:(η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate
CAS No.:206051-68-5
Molecular Formula:C₁₀H₁₅Sn*C₂₄BF₂₀
Molecular Weight:932.982
Hs Code.:

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Chemical Property of (η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate

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Technology Process of (η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate

There total 1 articles about (η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 187038-29-5
(pentamethylcyclopentadienyl)tin chloride

: 2797-28-6
lithium tetrakis(pentafluorophenyl)borate

: 206051-68-5
(η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate

Guidance literature:: In dichloromethane; byproducts: LiCl; stirring (room temp., overnight); filtering, evapn., extg. (CHCl3), recrystn. (CH2Cl2 / hexane); elem. anal.;
DOI:10.1021/om980153j

Reference yield: 74.8%

: 68757-81-3
bis(pentamethylcyclopentadienyl)Sn

: 206051-68-5
(η(5)-pentamethylcyclopentadienyl)tin tetrakis(pentafluorophenyl)borate

: trans-[(Cp*Sn)2(μ-η5-η5-Cp*)][B(C6F5)4]

Guidance literature:: In dichloromethane; byproducts: LiCl; under Ar atm. soln. (Cp*Sn)(B(C6F5)4) in CH2Cl2 was added to stirred soln. Cp*2Sn in CH2Cl2 at 0°C, warmed slowly to room temp., stirred overnight; mixt. was filtered through Celite, soln. was concd. in vac. and layered with hexane;
DOI:10.1039/b510337a