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Technology Process of CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13

CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13

Base Information
  • Chemical Name:CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13
  • CAS No.:1082577-56-7
  • Molecular Formula:C31H35BS2
  • Molecular Weight:482.562
  • Hs Code.:
CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>B(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)C<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>C<sub>6</sub>H<sub>13</sub>

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Chemical Property of CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13
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Technology Process of CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13

There total 1 articles about CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>BBrC<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>C<sub>6</sub>H<sub>13</sub>
1082577-52-3

CH2CHC6H4BBrC4H2S2C4H2C6H13

(Cu(mesitylene))*(Toluene)<sub>0.2</sub>

(Cu(mesitylene))*(Toluene)0.2

CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>B(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)C<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>C<sub>6</sub>H<sub>13</sub>
1082577-56-7

CH2CHC6H4B(C6H2(CH3)3)C4H2S2C4H2C6H13

Guidance literature:
In toluene; Cu-compound in toluene was added dropwise to a soln. of B-compound in toluene, the mixt. was allowed to react for 3 h then refluxed for 72 h; filtered through celite, concd., pptd. into cold hexane, repeated pptn. from toluene into hexane, dried at 50°C under high vac.; elem. anal.;
DOI:10.1021/ja063302v
upstream raw materials:

CH2CHC6H4BBrC4H2S2C4H2C6H13

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