n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

Base Information

Chemical Name:n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate
CAS No.:125655-58-5
Molecular Formula:C₃₈H₃₄N₆O₄
Molecular Weight:638.726
Hs Code.:

n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

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Chemical Property of n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

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Technology Process of n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

There total 5 articles about n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 125655-55-2
n-propyl α-cyano-4-<2-(4-pyrimidyl)ethenyl>cinnamate

: 125655-58-5
n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

Guidance literature:: Ambient temperature; Irradiation;

Reference yield: 6.0%

: 125655-55-2
n-propyl α-cyano-4-<2-(4-pyrimidyl)ethenyl>cinnamate

: 125655-58-5
n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

: 134747-68-5
C₃₈H₃₄N₆O₄

Guidance literature:: at -40 ℃; for 1h; Product distribution; Mechanism; Irradiation; variation of temperature and wave-length;

Reference yield:

: 3438-46-8
4-Methylpyrimidine

: 125655-58-5
n-propyl 1-cyano-3-<4-<2-cyano-2-(n-propyloxycarbonyl)ethenyl>phenyl>-2-<4-<2-(4-pyrimidyl)ethenyl>phenyl>-4-(4-pyrimidyl)-1-cyclobutanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / acetic anhydride; acetic acid / 4 h / Heating

2: 71 percent / piperidine / 7 h / Heating

3: Nikkol TL-10FF surfactant / H₂O / Irradiation

With piperidine; Nikkol TL-10FF surfactant; In water; acetic anhydride; acetic acid;
DOI:10.1246/bcsj.62.1556