Technology Process of C47H63N5O13
There total 11 articles about C47H63N5O13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NIS; AgOTF; 2,6-di-tert-butylpyridine / CH2Cl2 / -78 - 20 °C
2: piperidine / dimethylformamide
With
piperidine; N-iodo-succinimide; 2,6-di-tert-butyl-pyridine; silver trifluoromethanesulfonate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2005.01.023
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: MeOH / 65 °C
2.1: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
2.2: 55 percent / silica gel; MeOH / 65 °C
3.1: NIS; AgOTF; 2,6-di-tert-butylpyridine / CH2Cl2 / -78 - 20 °C
4.1: piperidine / dimethylformamide
With
piperidine; methanol; N-iodo-succinimide; 2,6-di-tert-butyl-pyridine; oxalyl dichloride; silver trifluoromethanesulfonate; dimethyl sulfoxide; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
2.1: Swern oxidation;
DOI:10.1016/j.tetlet.2005.01.023
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: (COCl)2; DMSO; Et3N / CH2Cl2 / -78 - 20 °C
1.2: 55 percent / silica gel; MeOH / 65 °C
2.1: NIS; AgOTF; 2,6-di-tert-butylpyridine / CH2Cl2 / -78 - 20 °C
3.1: piperidine / dimethylformamide
With
piperidine; N-iodo-succinimide; 2,6-di-tert-butyl-pyridine; oxalyl dichloride; silver trifluoromethanesulfonate; dimethyl sulfoxide; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
1.1: Swern oxidation;
DOI:10.1016/j.tetlet.2005.01.023
