gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid

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Chemical Name:gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid
CAS No.:1085268-55-8
Molecular Formula:C₃₆H₄₆GdN₇O₇
Molecular Weight:846.054
Hs Code.:

gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid

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Chemical Property of gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid

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Technology Process of gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid

There total 1 articles about gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: gadolinium(III) chloride hexahydrate

: 1083157-94-1
(4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis[(tert-butoxycarbonyl)methyl]-1,4,7,10-tetraazacyclododec-1-yl)acetic acid tert-butyl ester

: 1085268-55-8
gadolinium(III) (4-(3-[2-[bis(pyridin-2-ylmethyl)amino]-3-methylphenoxy]propyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl)acetic acid

Guidance literature:: With sodium hydroxide; trifluoroacetic acid; In water; trifluoroacetic acid; soln. of CF3CO2H (95 equiv.), H2O (2.5 equiv.) and triisopropylsilane (2.5 equiv.) added to ligand for 12 h; purged with air; Et2O added; centrifuged; decanted; washed (Et2O); brought up in H2O; NaOH added to pH 6.5;Gd salt (1.1 equiv.) added; stirred; NaOH added to pH 10; pelleted; chromd. (H2O/MeCN, from 0 to 100% over 35min); freeze-dried;
DOI:10.1021/ic801458u