benzamido-5-hydroxy-2-methoxyhexan-4-olide

Base Information

Chemical Name:benzamido-5-hydroxy-2-methoxyhexan-4-olide
CAS No.:101536-03-2
Molecular Formula:C₁₄H₁₇NO₅
Molecular Weight:279.293
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzamido-5-hydroxy-2-methoxyhexan-4-olide

Chemical Property:

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Technology Process of benzamido-5-hydroxy-2-methoxyhexan-4-olide

There total 10 articles about benzamido-5-hydroxy-2-methoxyhexan-4-olide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101535-99-3
cis-3-methoxy-4-(prop-1-enyl)azetidin-2-one

: 101536-03-2,101536-04-3
benzamido-5-hydroxy-2-methoxyhexan-4-olide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydoxide / methanol / Heating

2: potassium hydroxide / acetone; H₂O / 4 h / Ambient temperature

3: cc. H₂SO₄ / Heating

4: osmium tetraoxide, N-methylmorpholine N-oxide / acetone; H₂O / 48 h

With potassium hydroxide; osmium(VIII) oxide; 4-methylmorpholine N-oxide; sulfuric acid; In methanol; water; acetone;

Reference yield:

: 101535-99-3
cis-3-methoxy-4-(prop-1-enyl)azetidin-2-one

: 101536-03-2,101536-04-3
benzamido-5-hydroxy-2-methoxyhexan-4-olide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydoxide / methanol / Heating

2: potassium hydroxide / acetone; H₂O / 4 h / Ambient temperature

3: cc. H₂SO₄ / Heating

4: osmium tetraoxide, N-methylmorpholine N-oxide / acetone; H₂O / 48 h

With potassium hydroxide; osmium(VIII) oxide; 4-methylmorpholine N-oxide; sulfuric acid; In methanol; water; acetone;

Reference yield:

: 101535-98-2
cis-3-methoxy-1-(4-methoxyphenyl)-4-(prop-1-enyl)azetidin-2-one

: 101536-03-2,101536-04-3
benzamido-5-hydroxy-2-methoxyhexan-4-olide

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / cerium(IV) ammonium nitrate / acetonitrile; H₂O / 1 h / 0 °C

2: potassium hydoxide / methanol / Heating

3: potassium hydroxide / acetone; H₂O / 4 h / Ambient temperature

4: cc. H₂SO₄ / Heating

5: osmium tetraoxide, N-methylmorpholine N-oxide / acetone; H₂O / 48 h

With potassium hydroxide; osmium(VIII) oxide; ammonium cerium(IV) nitrate; 4-methylmorpholine N-oxide; sulfuric acid; In methanol; water; acetone; acetonitrile;