Technology Process of C2HF3O2*C24H25N9O5S
There total 5 articles about C2HF3O2*C24H25N9O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H27N9O5S;
With
sodium hydroxide;
In
ethanol; water;
at 20 ℃;
for 2h;
trifluoroacetic acid;
In
acetonitrile;
DOI:10.1021/jm2011996
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine; copper(I) bromide / water; N,N-dimethyl-formamide / 0.08 h / 120 °C / Microwave irradiation
2: sodium hydroxide / ethanol; water / 2 h / 20 °C
With
N-ethyl-N,N-diisopropylamine; copper(I) bromide; sodium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm2011996
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide / dimethyl sulfoxide / 2 h / 20 °C
2: N-ethyl-N,N-diisopropylamine; copper(I) bromide / water; N,N-dimethyl-formamide / 0.08 h / 120 °C / Microwave irradiation
3: sodium hydroxide / ethanol; water / 2 h / 20 °C
With
sodium azide; N-ethyl-N,N-diisopropylamine; copper(I) bromide; sodium hydroxide;
In
ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm2011996