C₄₀H₆₃N₃O₉Si

Base Information

Chemical Name:C₄₀H₆₃N₃O₉Si
CAS No.:1255213-31-0
Molecular Formula:C₄₀H₆₃N₃O₉Si
Molecular Weight:758.04
Hs Code.:

C<sub>40</sub>H<sub>63</sub>N<sub>3</sub>O<sub>9</sub>Si

Synonyms:

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Chemical Property of C₄₀H₆₃N₃O₉Si

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Technology Process of C₄₀H₆₃N₃O₉Si

There total 13 articles about C₄₀H₆₃N₃O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1255213-21-8
(S)-methyl 5-nitro-2-(pent-4-en-2-yloxy)benzoate

: 1255213-31-0
C₄₀H₆₃N₃O₉Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 23 h

1.2: pH 1

2.1: thionyl chloride / 2 h / 85 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

With thionyl chloride; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja105119r

Reference yield:

: 1255213-22-9
C₁₂H₁₃NO₅

: 1255213-31-0
C₄₀H₆₃N₃O₉Si

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / 85 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ja105119r

Reference yield:

: 1255212-57-7
(1R,2S)-1-phenyl-2-(N,2,4,6-tetramethylphenylsulfonamido)propyl (2R,3S)-4-(tert-butoxycarbonyl(methyl)amino)-3-hydroxy-2-methylbutanoate

: 1255213-31-0
C₄₀H₆₃N₃O₉Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; dihydrogen peroxide; sodium hydroxide / methanol; tert-butyl alcohol / 0 - 20 °C

1.2: pH 4

2.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 65 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; dimethylsulfide borane complex; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ja105119r