C₂₀H₁₅ClF₈N₆OS

Base Information

Chemical Name:C₂₀H₁₅ClF₈N₆OS
CAS No.:1393095-46-9
Molecular Formula:C₂₀H₁₅ClF₈N₆OS
Molecular Weight:574.885
Hs Code.:

C<sub>20</sub>H<sub>15</sub>ClF<sub>8</sub>N<sub>6</sub>OS

Synonyms:

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Chemical Property of C₂₀H₁₅ClF₈N₆OS

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Technology Process of C₂₀H₁₅ClF₈N₆OS

There total 4 articles about C₂₀H₁₅ClF₈N₆OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 251085-87-7
methyl 5-bromo-2-chloro-benzoate

: 1393095-46-9
C₂₀H₁₅ClF₈N₆OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / triphenylphosphine; palladium diacetate / Inert atmosphere; Reflux

1.2: 1 h

2.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

3.1: water; lithium hydroxide / tetrahydrofuran / 5 h / 60 °C

4.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 50 °C

With water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; copper(ll) sulfate pentahydrate; palladium diacetate; sodium L-ascorbate; triphenylphosphine; In tetrahydrofuran; ISOPROPYLAMIDE; water; tert-butyl alcohol;

Reference yield:

: 792912-10-8
2-chloro-5-ethynyl-benzoic acid methyl ester

: 1393095-46-9
C₂₀H₁₅ClF₈N₆OS

Guidance literature:: Multi-step reaction with 3 steps

1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

2: water; lithium hydroxide / tetrahydrofuran / 5 h / 60 °C

3: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 50 °C

With water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; ISOPROPYLAMIDE; water; tert-butyl alcohol;

Reference yield:

: 104315-28-8
5-fluoro-1-methyl-3-(1,1,2,2,2-pentafluoroethyl)-4-(trifluoromethyl)pyrazole

: 1393095-46-9
C₂₀H₁₅ClF₈N₆OS

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / dimethyl sulfoxide / 20 °C

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

3: water; lithium hydroxide / tetrahydrofuran / 5 h / 60 °C

4: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 50 °C

With sodium azide; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; ISOPROPYLAMIDE; water; dimethyl sulfoxide; tert-butyl alcohol;