W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiCl₂C₆H₅

Base Information

• Chemical Name: W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiCl₂C₆H₅
• CAS No.: 1292301-76-8
• Molecular Formula: C₂₄H₄₀Cl₂N₂SiW
• Molecular Weight: 639.437
• Mol file: 1292301-76-8.mol

Synonyms:

Chemical Property of W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiCl₂C₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiCl₂C₆H₅

There total 1 articles about W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiCl₂C₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

W(C5(CH3)5)(CH3C(NCH(CH3)2)2)H3SiClHC6H5 (1292301-72-4) + W(C5(CH3)5)(CH3C(NCH(CH3)2)2)H3SiClHC6H4CH3 (1292301-73-5) → W(C5(CH3)5)(CH3C(NCH(CH3)2)2)H3SiCl2C6H5 (1292301-76-8)

Guidance literature:

In toluene; N2, Schlenk technique or glovebox; to soln. of W-complex silane added, stirred at 80 °C for 24 h; soln. evacuated to dryness, residue dissolved in pentane, filtered through Celite, concd., cooled to -35 °C, ppt. isolated by decantation, dried (vac.); elem. anal.;

DOI:10.1016/j.jorganchem.2010.11.046

upstream raw materials:

W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiClHC₆H₅

W(C₅(CH₃)5)(CH₃C(NCH(CH₃)2)2)H₃SiClHC₆H₄CH₃