Technology Process of C28H26ClFN4O3S2
There total 7 articles about C28H26ClFN4O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
carbon disulfide; C22H18ClFN4O;
With
triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.75h;
2-bromo-2-(2-ethyl)dioxolane;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1002/ardp.201200267
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methylamine / methanol / 20 °C
2.1: triethylamine / N,N-dimethyl-formamide / 0.75 h / 20 °C
2.2: 20 °C
With
triethylamine; methylamine;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1002/ardp.201200267
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 4 h / Reflux
2.1: thionyl chloride / N,N-dimethyl-formamide / 6 h / Reflux
3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 0.5 h / Reflux
4.1: acetone / 1 h / Reflux
5.1: isopropyl alcohol / 3 h / Reflux
6.1: methylamine / methanol / 20 °C
7.1: triethylamine / N,N-dimethyl-formamide / 0.75 h / 20 °C
7.2: 20 °C
With
N-Bromosuccinimide; thionyl chloride; triethylamine; methylamine; dibenzoyl peroxide;
In
methanol; tetrachloromethane; N,N-dimethyl-formamide; isopropyl alcohol; acetone;
DOI:10.1002/ardp.201200267