C₂₃H₂₆O₅

Base Information

Chemical Name:C₂₃H₂₆O₅
CAS No.:96949-09-6
Molecular Formula:C₂₃H₂₆O₅
Molecular Weight:382.456
Hs Code.:

C<sub>23</sub>H<sub>26</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₃H₂₆O₅

Chemical Property:

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Technology Process of C₂₃H₂₆O₅

There total 8 articles about C₂₃H₂₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39482-46-7
2,2-dimethylpent-4-enoyl chloride

: 96949-09-6,123238-64-2
C₂₃H₂₆O₅

Guidance literature:: Multi-step reaction with 7 steps

1: 96 percent / pyridine; CHCl₃ / 0 d3g C to room temp.

2: 98 percent / tetrahydrofuran / -78 °C

3: 100 percent / LiAlH₄, darvonalcohol-complex / diethyl ether / -100 °C

4: 82 percent / NaH, Bu₄NI / tetrahydrofuran / Ambient temperature

5: 81 percent / Pd(OAc)2, N,N'-bis(benzyliden)ethylendiamine / benzene / 70 °C

6: 2) DBU / 1) benzene, 80 deg C; 2) benzene, r.t.

7: 1) tetrabutylammoniumfluoride; 2) disiamylborane / 1) THF, r. t.; 2) ether

With palladium diacetate; lithium aluminium tetrahydride; N,N'-bis(benzyliden)ethylendiamine; darvonalcohol-; tetrabutyl ammonium fluoride; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; pyridine; diethyl ether; chloroform; benzene;

Reference yield:

: 123169-36-8
N-methoxy-N,2,2-trimethyl-4-pentenecarboxamide

: 96949-09-6,123238-64-2
C₂₃H₂₆O₅

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / tetrahydrofuran / -78 °C

2: 100 percent / LiAlH₄, darvonalcohol-complex / diethyl ether / -100 °C

3: 82 percent / NaH, Bu₄NI / tetrahydrofuran / Ambient temperature

4: 81 percent / Pd(OAc)2, N,N'-bis(benzyliden)ethylendiamine / benzene / 70 °C

5: 2) DBU / 1) benzene, 80 deg C; 2) benzene, r.t.

6: 1) tetrabutylammoniumfluoride; 2) disiamylborane / 1) THF, r. t.; 2) ether

With palladium diacetate; lithium aluminium tetrahydride; N,N'-bis(benzyliden)ethylendiamine; darvonalcohol-; tetrabutyl ammonium fluoride; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; diethyl ether; benzene;

Reference yield:

: 123169-38-0
(R)-1-(tert-Butyl-dimethyl-silanyloxy)-5,5-dimethyl-oct-7-en-2-yn-4-ol

: 96949-09-6,123238-64-2
C₂₃H₂₆O₅

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / NaH, Bu₄NI / tetrahydrofuran / Ambient temperature

2: 81 percent / Pd(OAc)2, N,N'-bis(benzyliden)ethylendiamine / benzene / 70 °C

3: 2) DBU / 1) benzene, 80 deg C; 2) benzene, r.t.

4: 1) tetrabutylammoniumfluoride; 2) disiamylborane / 1) THF, r. t.; 2) ether

With palladium diacetate; N,N'-bis(benzyliden)ethylendiamine; tetrabutyl ammonium fluoride; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; benzene;