C₃₃H₃₈N₂O₄

Base Information

Chemical Name:C₃₃H₃₈N₂O₄
CAS No.:1447825-58-2
Molecular Formula:C₃₃H₃₈N₂O₄
Molecular Weight:526.676
Hs Code.:

C<sub>33</sub>H<sub>38</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₃H₃₈N₂O₄

Chemical Property:

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Technology Process of C₃₃H₃₈N₂O₄

There total 14 articles about C₃₃H₃₈N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1013331-17-3
C₁₃H₂₀O₅

: C₂₅H₂₈N₂O

: 1447825-58-2
C₃₃H₃₈N₂O₄

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 19h;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-68-4
C₃₃H₃₉NO₄Si

: 1447825-58-2
C₃₃H₃₈N₂O₄

Guidance literature:: Multi-step reaction with 13 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.33 h / -78 °C

1.2: 1 h / 20 °C

2.1: copper(II) sulfate / dichloromethane / 22 h / 20 °C

3.1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

4.1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

5.1: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

8.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

9.1: 29 h / Reflux

10.1: potassium carbonate / methanol / 14 h / 20 °C

11.1: triethylamine / dichloromethane / 2 h / 0 °C

12.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

13.1: triethylamine / dichloromethane / 19 h / 0 - 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol; 3.1: |Grignard Reaction / 6.1: |Dess-Martin Oxidation / 9.1: |Curtius Rearrangement;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-71-9
C₃₅H₄₉NO₂SSi

: 1447825-58-2
C₃₃H₃₈N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

2: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

4: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

6: 29 h / Reflux

7: potassium carbonate / methanol / 14 h / 20 °C

8: triethylamine / dichloromethane / 2 h / 0 °C

9: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

10: triethylamine / dichloromethane / 19 h / 0 - 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 3: |Dess-Martin Oxidation / 6: |Curtius Rearrangement;
DOI:10.1021/jm400542h