benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate

Base Information

• Chemical Name: benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate
• CAS No.: 1354943-80-8
• Molecular Formula: C₄₈H₈₈NO₆P
• Molecular Weight: 806.204
• Mol file: 1354943-80-8.mol

Synonyms:

Chemical Property of benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate

There total 4 articles about benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C48H88NO5P → benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate (1354943-80-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1039/c2cc16827h

Reference yield:

1-Hexadecanol (36653-82-4,124-29-8) → benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate (1354943-80-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium hydride / mineral oil / 0.5 h / 100 °C / Inert atmosphere

1.2: 100 °C / Inert atmosphere

2.1: triethylamine / tetrahydrofuran / 4.33 h / 0 - 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

With sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; mineral oil;

DOI:10.1039/c2cc16827h

Reference yield:

1,3-bis(hexadecyloxy)propan-2-ol (14690-01-8) → benzyl (1,3-bis(hexadecyloxy)propan-2-yl)(2-(methyl(prop-2-yn-1-yl)amino)ethyl)phosphate (1354943-80-8)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 4.33 h / 0 - 20 °C / Inert atmosphere

2: tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;

DOI:10.1039/c2cc16827h

upstream raw materials:

1-Hexadecanol

1,3-bis(hexadecyloxy)propan-2-ol