Technology Process of C26H28N4O4S2
There total 11 articles about C26H28N4O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 28 percent / K2CrO4 / acetic acid; acetic anhydride / 1.) 2 h, room temperature, 2.) 4 h, 40 deg C, 3.) 4 d, room temperature
2: conc. hydrochloric acid / methanol
With
hydrogenchloride; potassium chromate;
In
methanol; acetic anhydride; acetic acid;
DOI:10.1021/jo00292a040
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.48 g / NaOH / ethanol / 3 h / Ambient temperature
2: 28 percent / K2CrO4 / acetic acid; acetic anhydride / 1.) 2 h, room temperature, 2.) 4 h, 40 deg C, 3.) 4 d, room temperature
3: conc. hydrochloric acid / methanol
With
hydrogenchloride; sodium hydroxide; potassium chromate;
In
methanol; ethanol; acetic anhydride; acetic acid;
DOI:10.1021/jo00292a040
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 96 percent / p-toluenesulfonic acid monohydrate / CH2Cl2 / 192 h / Ambient temperature
2: 97 percent / LiAlH4 / diethyl ether / 0.5 h
3: 3.26 g / pyridinium chlorochromate / CH2Cl2 / 0.42 h
4: 2.34 g / pyridinium p-toluenesulfonate / acetone; H2O / 1.5 h / Heating
5: 1.48 g / NaOH / ethanol / 3 h / Ambient temperature
6: 28 percent / K2CrO4 / acetic acid; acetic anhydride / 1.) 2 h, room temperature, 2.) 4 h, 40 deg C, 3.) 4 d, room temperature
7: conc. hydrochloric acid / methanol
With
hydrogenchloride; sodium hydroxide; potassium chromate; lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
methanol; diethyl ether; ethanol; dichloromethane; water; acetic anhydride; acetic acid; acetone;
DOI:10.1021/jo00292a040