C₉H₁₂BIO₃

Base Information

• Chemical Name: C₉H₁₂BIO₃
• CAS No.: 1557159-95-1
• Molecular Formula: C₉H₁₂BIO₃
• Molecular Weight: 305.908
• Mol file: 1557159-95-1.mol

Synonyms:

Chemical Property of C₉H₁₂BIO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₁₂BIO₃

There total 1 articles about C₉H₁₂BIO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

borane-THF (14044-65-6) + 1-(allyloxy)-4-iodobenzene (13997-71-2) + water (7732-18-5) → C9H12BIO3 (1557159-95-1)

Guidance literature:

borane-THF; 1-(allyloxy)-4-iodobenzene; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

water; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1021/ja413208y

Reference yield:

C9H12BIO3 (1557159-95-1) → 1-iodo-4-((5-phenylpent-4-yn-1-yl)oxy)benzene (875467-49-5)

Guidance literature:

Multi-step reaction with 2 steps

1: water; methanol / 2 h / 20 °C

2: tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; hydroxybenziodoxole; sodium carbonate / dichloromethane; water / 15 h / Inert atmosphere

With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; hydroxybenziodoxole; sodium carbonate; In methanol; dichloromethane; water;

DOI:10.1021/ja413208y

Reference yield:

potassium hydrogen difluoride + C9H12BIO3 (1557159-95-1) → potassium (3-(4-iodophenoxy)propyl)trifluoroborate (1557201-19-0)

Guidance literature:

In methanol; water; at 20 ℃; for 2h;

DOI:10.1021/ja413208y

upstream raw materials:

borane-THF

1-(allyloxy)-4-iodobenzene

water

Downstream raw materials:

potassium (3-(4-iodophenoxy)propyl)trifluoroborate

1-iodo-4-((5-phenylpent-4-yn-1-yl)oxy)benzene