1,4-Benzene diammonium iodide

Base Information

• Chemical Name: 1,4-Benzene diammonium iodide
• CAS No.: 116469-02-4
• Molecular Formula: C₆H₈N₂*HI
• Molecular Weight: 236.055
• Mol file: 116469-02-4.mol

Synonyms:

Chemical Property of 1,4-Benzene diammonium iodide

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,4-Phenylenediamine Dihydriodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-Benzene diammonium iodide

There total 2 articles about 1,4-Benzene diammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

{Mo(tris(3,5-dimethylpyrazolyl)borate)(NO)I2} + 1,4-phenylenediamine (106-50-3) → {Mo(tris(3,5-dimethylpyrazolyl)borate)(NO)I(p-NHC6H4NH2)}*0.5CH2Cl2 + NH2C6H4NH2*HI (56502-46-6,116469-02-4)

Guidance literature:

In dichloromethane; under N2, stirred at room temp. for 90 min; filtration (C6H8N2*HI), addn. of hexane to the filtrate, evapn. in vac., filtered off, recrystn. (CH2Cl2-diethyl ether); elem. anal.;

Reference yield:

1,4-phenylenediamine (106-50-3) → para-phenylenediammonium diiodide (116469-02-4)

Guidance literature:

With hydrogen iodide; In methanol; water; at 20 ℃; for 3h; Cooling with ice;

DOI:10.1002/adfm.202002366

upstream raw materials:

1,4-phenylenediamine