Technology Process of C29H35NO4Si
There total 4 articles about C29H35NO4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H27NO2Si;
With
lithium chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 - 22 ℃;
Inert atmosphere;
C11H9BrO2;
In
tetrahydrofuran;
at -78 ℃;
for 0.166667h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1021/jall0192b
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dimethyl zinc(II) / toluene / 0.5 h / 22 °C / Inert atmosphere
1.2: 0.5 h / 22 - 70 °C / Inert atmosphere
1.3: 12 h / 0 - 22 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; toluene / 0.08 h / 0 °C / Inert atmosphere
2.2: 2 h / 0 - 22 °C / Inert atmosphere
3.1: hydrogenchloride; water / methanol / 4 h / 22 °C / in air
4.1: triethylamine / tetrahydrofuran / 22 °C / Inert atmosphere
5.1: lithium bromide / tetrahydrofuran / 12 h / 22 °C / Inert atmosphere
6.1: lithium chloride; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 22 °C / Inert atmosphere
6.2: 0.17 h / -78 °C / Inert atmosphere
With
hydrogenchloride; water; dimethyl zinc(II); sodium hydride; triethylamine; lithium chloride; lithium bromide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jall0192b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium bromide / tetrahydrofuran / 12 h / 22 °C / Inert atmosphere
2.1: lithium chloride; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 22 °C / Inert atmosphere
2.2: 0.17 h / -78 °C / Inert atmosphere
With
lithium chloride; lithium bromide; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1021/jall0192b
