tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone

Base Information

Chemical Name:tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone
CAS No.:157458-87-2
Molecular Formula:C₂₄H₄₂BFN₂
Molecular Weight:388.42
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone

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Technology Process of tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone

There total 1 articles about tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 129161-76-8
2,4,6-tri-t-butylphenyldifluoroborane

: 29443-45-6
3,3-Dimethyl-2-butanone hydrazone

: 157458-87-2
tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone

Guidance literature:: With n-butyllithium; In hexane; byproducts: LiF; addn. of C4H9Li to a soln. of the ketonehydrazone at room temperature; reflux for 1 h; addn. of the Li-salt to the starting borane at 0 ° C; stirring for 12 h;; distillation; crystn.; elem. anal.;;

Reference yield: 43.0%

: 157458-87-2
tert-butylmehylketone-(2,4,6-tri-tert-butylphenyl-fluoroboryl)-hydrazone

: 5,7-bis(2,4,6-tri-tert-butylphenyl)-3-tert-butyl-6-(2,2-dimethyl-butanimine)-1,2,6-triaza-5,7-diboracyclohept-3-ene=5,7-Bis(2,4,6-tri-tert-butylphenyl)-3-tert-butyl-6-(2,2-dimethyl-butanimin)-1,2,6-triaza-5,7-diboracyclohept-3-en

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; hexane; byproducts: LiF; addn. of t-C4H9Li to a soln. of the borylhydrazone in hexane/THF at -50 ° C;; solvent removal; work up under reduced pressure at 100 ° C; sublimation at 170 ° C/0.01 mbar; elem. anal.;;