Technology Process of C30H32O4
There total 3 articles about C30H32O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 3h;
Overall yield = 98%; Overall yield = 44 mg; enantioselective reaction;
DOI:10.1002/anie.201208349
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: C44H77NO4Si2; salicylic acid / 1,4-dioxane / 20 h / 50 °C
1.2: 0.5 h / 0 °C / Molecular sieve
2.1: 3-chloro-benzenecarboperoxoic acid; potassium carbonate / methanol / 0.5 h / 0 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C
With
palladium 10% on activated carbon; C44H77NO4Si2; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; salicylic acid;
In
1,4-dioxane; methanol;
1.1: |Diels-Alder Cycloaddition / 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/anie.201208349
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: C44H77NO4Si2; salicylic acid / 1,4-dioxane / 20 h / 50 °C
1.2: 0.5 h / 0 °C / Molecular sieve
2.1: 3-chloro-benzenecarboperoxoic acid; potassium carbonate / methanol / 0.5 h / 0 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C
With
palladium 10% on activated carbon; C44H77NO4Si2; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; salicylic acid;
In
1,4-dioxane; methanol;
1.1: |Diels-Alder Cycloaddition / 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/anie.201208349
