Stannane, tributyl(4-phenyl-1-butenyl)-, (Z)-

Base Information

Chemical Name:Stannane, tributyl(4-phenyl-1-butenyl)-, (Z)-
CAS No.:138034-95-4
Molecular Formula:C₂₂H₃₈Sn
Molecular Weight:421.254
Hs Code.:
Mol file:138034-95-4.mol

Synonyms:

Suppliers and Price of Stannane, tributyl(4-phenyl-1-butenyl)-, (Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Stannane, tributyl(4-phenyl-1-butenyl)-, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Stannane, tributyl(4-phenyl-1-butenyl)-, (Z)-

There total 5 articles about Stannane, tributyl(4-phenyl-1-butenyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 184370-64-7
(4-bromobut-3-yn-1-yl)benzene

: 688-73-3
tri-n-butyl-tin hydride

: 138034-95-4,138034-96-5
(C₆H₅C₂H₄)(H)C₂(H)Sn(C₄H₉)3

Guidance literature:: With triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; Sn-compd. addn. to stirred soln. of components and catalyst (room temp.,N2), stirring 2 h, quenching with satd. aq. KF, vigorous stirring overn ight, light petroleum addn., org. layer sepn., washing (water, brine), org. layer evapn. to dryness; residue chromy. (SiO2, Et2O/light petroleum 5:95), ratio E/Z>95:5;
DOI:10.1039/p19960002417

Reference yield: 5.0%

: 218902-80-8
(4,4-diiodoobut-3-enyl)benzene

: 768-56-9
4-Phenylbut-1-ene

: 218902-81-9
(Z)-(4-iodobut-3-en-1-yl)benzene

: 138034-95-4,138034-96-5
tributyl(4-phenylbut-1-en-1-yl)stannane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; In benzene; for 0.25h; Ambient temperature;
DOI:10.1021/jo9812781

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 138034-95-4,138034-96-5
tributyl(4-phenylbut-1-en-1-yl)stannane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) PPh₃ / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) CH₂Cl₂, 0 deg C (10 min), room temperature, 15 min

2: 11 percent / Pd(PPh₃)4, Bu₃SnH / benzene / 0.25 h / Ambient temperature

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; triphenylphosphine; In benzene;
DOI:10.1021/jo9812781