Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)⁽¹⁺⁾*PF₆^(1-) = [Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)]PF₆

Base Information

• Chemical Name: Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)⁽¹⁺⁾*PF₆^(1-) = [Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)]PF₆
• CAS No.: 102533-38-0
• Molecular Formula: C₅₅H₅₃Cl₃NP₄Re₂*F₆P
• Molecular Weight: 1475.66

Synonyms:

Chemical Property of Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)⁽¹⁺⁾*PF₆^(1-) = [Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)]PF₆

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Technology Process of Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)⁽¹⁺⁾*PF₆^(1-) = [Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)]PF₆

There total 1 articles about Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)⁽¹⁺⁾*PF₆^(1-) = [Re₂Cl₃((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2(NCC₂H₅)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Re2Cl3((C6H5)2PCH2CH2P(C6H5)2)2(NCC2H5)(2+)*2PF6(1-) = [Re2Cl3((C6H5)2PCH2CH2P(C6H5)2)2(NCC2H5)][PF6]2 → Re2Cl3((C6H5)2PCH2CH2P(C6H5)2)2(NCC2H5)(1+)*PF6(1-) = [Re2Cl3((C6H5)2PCH2CH2P(C6H5)2)2(NCC2H5)]PF6 (102533-38-0)

Guidance literature:

With Li[B(C₂H₅)3H]; In tetrahydrofuran; (N2), soln. of the Re-complex treated with a soln. of LiBEt3H, stirred at room temp. for minutes, stirred for 0.5 h (after change of color); pptd. by addn. of Et2O, recrystd. from CH2Cl2/Et2O, collected, washed with Et2O, dried in vacuo, elem. anal.;

DOI:10.1039/DT9860000055

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