3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

Base Information

Chemical Name:3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose
CAS No.:97119-19-2
Molecular Formula:C₄₁H₄₉NO₁₂
Molecular Weight:751.808
Hs Code.:

3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-<D2>benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

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Chemical Property of 3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

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Technology Process of 3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

There total 16 articles about 3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108-24-7
acetic anhydride

: 97119-13-6
3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,7-tri-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-2-O-benzyl-4-desoxy-β-D-glucopyranose

: 97119-19-2
3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

Guidance literature:: With boron trifluoride diethyl etherate; for 4h;

Reference yield:

: 86845-47-8,86853-27-2
1L-1-Desoxy-1-C-hydroxymethyl-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-19-2
3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 10 steps

1: 94 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

2: 81 percent / 98percent acetic acid / 30 °C

3: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

4: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

5: 89 percent / pyridine / CH₂Cl₂ / -40 °C

6: 69 percent / NaN₃ / hexamethylphosphoric acid triamide / 30 °C

7: 86 percent / 4percent NiCl₂-solution, NaBH₄ / ethanol

8: butan-1-ol / 30 h / 110 °C

9: pyridine / 40 °C

10: 89 percent / Et₂O-BF₃ / 4 h

With pyridine; sodium tetrahydroborate; sodium azide; boron trifluoride diethyl etherate; sodium hydride; acetic acid; nickel dichloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; water; N,N-dimethyl-formamide; butan-1-ol;

Reference yield:

: 86845-48-9,86853-28-3
1L-7-O-Acetyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-19-2
3-O-Acetyl-1,6-anhydro-2-O-benzyl-4-desoxy-4-<1D-(1N,2,4/3,5,6)-<6,7-di-O-acetyl-2,3-di-O-benzyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 9 steps

1: 75 percent / 98percent acetic acid / 30 °C

2: 1) 1 N NaOCH₃, 2) NaH / 1) methanol, 1 h, 2) DMF, 2 h, 0 deg C; 5 h, room temp.

3: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

4: 89 percent / pyridine / CH₂Cl₂ / -40 °C

5: 69 percent / NaN₃ / hexamethylphosphoric acid triamide / 30 °C

6: 86 percent / 4percent NiCl₂-solution, NaBH₄ / ethanol

7: butan-1-ol / 30 h / 110 °C

8: pyridine / 40 °C

9: 89 percent / Et₂O-BF₃ / 4 h

With pyridine; sodium tetrahydroborate; sodium azide; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; acetic acid; nickel dichloride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; water; butan-1-ol;