4-Methyl-n-(7-nitro-9h-fluoren-2-yl)benzenesulfonamide

Base Information

• Chemical Name: 4-Methyl-n-(7-nitro-9h-fluoren-2-yl)benzenesulfonamide
• CAS No.: 70730-48-2
• Molecular Formula: C₂₀H₁₆N₂O₄S
• Molecular Weight: 380.424
• NSC Number: 141064
• DSSTox Substance ID: DTXSID90301093
• Wikidata: Q82044662
• Mol file: 70730-48-2.mol

Synonyms:4-methyl-n-(7-nitro-9h-fluoren-2-yl)benzenesulfonamide;70730-48-2;NSC141064;DTXSID90301093;NSC-141064

Chemical Property of 4-Methyl-n-(7-nitro-9h-fluoren-2-yl)benzenesulfonamide

Chemical Property:

• Vapor Pressure: 8.38E-14mmHg at 25°C
• Boiling Point: 587.9°C at 760 mmHg
• Flash Point: 309.4°C
• PSA: 100.37000
• Density: 1.432g/cm³
• LogP: 5.95220
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 380.08307817
• Heavy Atom Count: 27
• Complexity: 648

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)NC2=CC3=C(C=C2)C4=C(C3)C=C(C=C4)[N+](=O)[O-]

Technology Process of 4-Methyl-n-(7-nitro-9h-fluoren-2-yl)benzenesulfonamide

There total 1 articles about 4-Methyl-n-(7-nitro-9h-fluoren-2-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-7-nitrofluorene (1214-32-0) + p-toluenesulfonyl chloride (98-59-9) → N-(7-nitro-fluoren-2-yl)-toluene-4-sulfonamide (70730-48-2)

Guidance literature:

With pyridine;

DOI:10.1039/jr9490002020

Reference yield:

N-(7-nitro-fluoren-2-yl)-toluene-4-sulfonamide (70730-48-2) → N-(3,7-dinitro-fluoren-2-yl)-toluene-4-sulfonamide (102024-64-6)

Guidance literature:

With nitric acid; acetic acid;

DOI:10.1039/jr9490002020 DOI:10.1021/jo01075a017

Reference yield:

N-(7-nitro-fluoren-2-yl)-toluene-4-sulfonamide (70730-48-2) → N-(7-amino-fluoren-2-yl)-toluene-4-sulfonamide

Guidance literature:

With ethanol; calcium chloride; zinc;

upstream raw materials:

2-amino-7-nitrofluorene

p-toluenesulfonyl chloride

Downstream raw materials:

N-(3,7-dinitro-fluoren-2-yl)-toluene-4-sulfonamide