(R)-1-benzyloxy-3-methyl-7-pentadecyne

Base Information

Chemical Name:(R)-1-benzyloxy-3-methyl-7-pentadecyne
CAS No.:1446944-60-0
Molecular Formula:C₂₃H₃₆O
Molecular Weight:328.538
Hs Code.:

Synonyms:

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Chemical Property of (R)-1-benzyloxy-3-methyl-7-pentadecyne

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Technology Process of (R)-1-benzyloxy-3-methyl-7-pentadecyne

There total 7 articles about (R)-1-benzyloxy-3-methyl-7-pentadecyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3452-09-3
1-nonyne

: 1446944-59-7
(R)-6-benzyloxy-4-methylhexyl iodide

: 1446944-60-0
(R)-1-benzyloxy-3-methyl-7-pentadecyne

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; Reflux;
DOI:10.1271/bbb.120436

Reference yield:

: 1117-61-9
(3R)-citronellol

: 1446944-60-0
(R)-1-benzyloxy-3-methyl-7-pentadecyne

Guidance literature:: Multi-step reaction with 7 steps

1: potassium tert-butylate / dimethyl sulfoxide

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane

3: periodic acid dihydrate / tetrahydrofuran / 1 h / 0 - 20 °C

4: lithium aluminium tetrahydride / diethyl ether

5: pyridine

6: sodium iodide / N,N-dimethyl-formamide

7: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / Reflux

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; periodic acid dihydrate; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1271/bbb.120436

Reference yield:

: 2385-77-5
(R)-Citronellal

: 1446944-60-0
(R)-1-benzyloxy-3-methyl-7-pentadecyne

Guidance literature:: Multi-step reaction with 8 steps

1: lithium aluminium tetrahydride / diethyl ether

2: potassium tert-butylate / dimethyl sulfoxide

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane

4: periodic acid dihydrate / tetrahydrofuran / 1 h / 0 - 20 °C

5: lithium aluminium tetrahydride / diethyl ether

6: pyridine

7: sodium iodide / N,N-dimethyl-formamide

8: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / Reflux

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; periodic acid dihydrate; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1271/bbb.120436