Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy-2-[[(2-methoxy-1,1-dimethylethyl)imino ]methyl]-1-methyl-1-(phenylmethyl)-

Base Information

Chemical Name:Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy-2-[[(2-methoxy-1,1-dimethylethyl)imino ]methyl]-1-methyl-1-(phenylmethyl)-
CAS No.:138037-57-7
Molecular Formula:C₂₅H₃₄N₂O₃
Molecular Weight:410.557
Hs Code.:
Mol file:138037-57-7.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy-2-[[(2-methoxy-1,1-dimethylethyl)imino ]methyl]-1-methyl-1-(phenylmethyl)-

Chemical Property:

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Technology Process of Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy-2-[[(2-methoxy-1,1-dimethylethyl)imino ]methyl]-1-methyl-1-(phenylmethyl)-

There total 3 articles about Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy-2-[[(2-methoxy-1,1-dimethylethyl)imino ]methyl]-1-methyl-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138037-55-5
[1-((S)-6,7-Dimethoxy-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl)-meth-(E)-ylidene]-((S)-1-methoxymethyl-2-methyl-propyl)-amine

: 138037-57-7
[1-(1-Benzyl-6,7-dimethoxy-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl)-meth-(E)-ylidene]-(2-methoxy-1,1-dimethyl-ethyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: N₂H₄

3: s-BuLi / -100 °C / multistep reaction; determination of the configurational stability of the intermediate lithio-compound

With sec.-butyllithium; hydrazine;
DOI:10.1016/0040-4039(91)80069-I

Reference yield:

: 493-48-1
(S)-salsolidine

: 138037-57-7
[1-(1-Benzyl-6,7-dimethoxy-1-methyl-3,4-dihydro-1H-isoquinolin-2-yl)-meth-(E)-ylidene]-(2-methoxy-1,1-dimethyl-ethyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

2: s-BuLi / -100 °C / multistep reaction; determination of the configurational stability of the intermediate lithio-compound

With sec.-butyllithium;
DOI:10.1016/0040-4039(91)80069-I