Technology Process of C29H37BrO4
There total 9 articles about C29H37BrO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 89 percent / p-toluenesulfonic acid / benzene / 2 h / Heating
2: 88 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 3 h / Ambient temperature
4: 73 percent / NaH, tert-amyl alcohol / benzene / 1 h / Heating
5: 42 percent / tetrahydrofuran / 7 h / -78 °C / Irradiation
6: 93 percent / sodium borohydride / methanol / 0.67 h / Ambient temperature
7: pyridine / 16 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; tert-Amyl alcohol; sodium acetate; sodium hydride; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1139/v85-563
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 88 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 3 h / Ambient temperature
3: 73 percent / NaH, tert-amyl alcohol / benzene / 1 h / Heating
4: 42 percent / tetrahydrofuran / 7 h / -78 °C / Irradiation
5: 93 percent / sodium borohydride / methanol / 0.67 h / Ambient temperature
6: pyridine / 16 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; tert-Amyl alcohol; sodium acetate; sodium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.1139/v85-563
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / NaH, tert-amyl alcohol / benzene / 1 h / Heating
2: 42 percent / tetrahydrofuran / 7 h / -78 °C / Irradiation
3: 93 percent / sodium borohydride / methanol / 0.67 h / Ambient temperature
4: pyridine / 16 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; tert-Amyl alcohol; sodium hydride;
In
tetrahydrofuran; methanol; benzene;
DOI:10.1139/v85-563