Technology Process of 11-amino-5-acetyl-12-(p-bromobenzoyl)-5,6-dihydrodibenzofuro<2,3-d>azocine
There total 5 articles about 11-amino-5-acetyl-12-(p-bromobenzoyl)-5,6-dihydrodibenzofuro<2,3-d>azocine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
for 10h;
Heating;
DOI:10.1007/BF00633227
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent / sodium acetate / propan-2-ol / 1.5 h / Heating
2: 92.5 percent / sodium acetate / dioxane / 0.25 h / Heating
3: 73 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 1 h / Heating
4: 23 percent / potassium carbonate / acetone / 10 h / Heating
With
potassium tert-butylate; sodium acetate; potassium carbonate;
In
1,4-dioxane; isopropyl alcohol; acetone; tert-butyl alcohol;
DOI:10.1007/BF00633227
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92.5 percent / sodium acetate / dioxane / 0.25 h / Heating
2: 73 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 1 h / Heating
3: 23 percent / potassium carbonate / acetone / 10 h / Heating
With
potassium tert-butylate; sodium acetate; potassium carbonate;
In
1,4-dioxane; acetone; tert-butyl alcohol;
DOI:10.1007/BF00633227
