C₂₈H₂₇F₅O₆S

Base Information

Chemical Name:C₂₈H₂₇F₅O₆S
CAS No.:1382088-14-3
Molecular Formula:C₂₈H₂₇F₅O₆S
Molecular Weight:586.577
Hs Code.:

C<sub>28</sub>H<sub>27</sub>F<sub>5</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₂₈H₂₇F₅O₆S

Chemical Property:

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Technology Process of C₂₈H₂₇F₅O₆S

There total 21 articles about C₂₈H₂₇F₅O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1382088-13-2
C₂₁H₂₆O₅

: 1382088-14-3
C₂₈H₂₇F₅O₆S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / 1,4-dioxane; water / 6 h / 90 °C / Inert atmosphere

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 0.83 h / -78 - 20 °C

3: manganese(IV) oxide / chloroform / 20 °C

4: dmap / dichloromethane

With dmap; manganese(IV) oxide; sodium tetrahydroborate; cerium(III) chloride heptahydrate; sodium hydroxide; In 1,4-dioxane; methanol; dichloromethane; chloroform; water;
DOI:10.1021/jo3008034

Reference yield:

: 212185-22-3
(5R,6R)-6-(3,3-diethoxypropyl)-2,6-dimethyl-5-(1-methylethenyl)-2-cyclohexen-1-one

: 1382088-14-3
C₂₈H₂₇F₅O₆S

Guidance literature:: Multi-step reaction with 21 steps

1: dihydrogen peroxide; sodium hydroxide

2: cerium(III) chloride heptahydrate; sodium hypochlorite solution / dichloromethane; water / 0 °C

3: N-ethylmorpholine N-oxide; lithium iodide / N,N-dimethyl-formamide / 30 h / 55 °C

4: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 3 h / 0 °C

5: 0 °C

6: pyridinium p-toluenesulfonate / acetone / 45 °C

7: dichloromethane / 36 h / 28 °C / Inert atmosphere

8: triethylamine / dichloromethane / -78 °C

9: 2,6-di-tert-butyl-4-methyl-phenol / toluene; methyloxirane / 96 h / 140 °C / Inert atmosphere

10: diethylzinc / hexane; toluene / 4 h / 0 °C

11: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / -30 - 20 °C

12: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 °C

13: 2,2,6,6-tetramethyl-piperidine; n-butyllithium; diethylaluminium chloride / hexane; toluene / 1.33 h / 0 °C

14: Grubbs catalyst first generation; p-benzoquinone / dichloromethane / 1 h / Reflux

15: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 20 °C / Inert atmosphere

16: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / Molecular sieve

17: fluorosilicic acid / water; acetonitrile / 18 h / 0 - 4 °C

18: sodium hydroxide / 1,4-dioxane; water / 6 h / 90 °C / Inert atmosphere

19: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 0.83 h / -78 - 20 °C

20: manganese(IV) oxide / chloroform / 20 °C

21: dmap / dichloromethane

With 2,2,6,6-tetramethyl-piperidine; Grubbs catalyst first generation; dmap; manganese(IV) oxide; sodium chlorite; sodium tetrahydroborate; n-butyllithium; N-ethylmorpholine N-oxide; sodium hypochlorite solution; tetrapropylammonium perruthennate; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; cerium(III) chloride heptahydrate; 2,6-di-tert-butyl-4-methyl-phenol; fluorosilicic acid; dihydrogen peroxide; diethylzinc; diethylaluminium chloride; pyridinium p-toluenesulfonate; sodium hydride; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; p-benzoquinone; sodium hydroxide; lithium iodide; In 1,4-dioxane; methanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; methyloxirane; mineral oil; tert-butyl alcohol; benzene;
DOI:10.1021/jo3008034

Reference yield:

: 1382087-95-7
(1aS,1bS,3aR,4S,4aR,5aS,6aS,6bS,8aR)-methyl 8a-((tert-butyldimethylsilyl)oxy)-4-hydroxy-1a,3a,4a-trimethyltetradecahydro-1H-cyclopropa[7,8]phenanthro[2,3-b]oxirene-6b-carboxylate

: 1382088-14-3
C₂₈H₂₇F₅O₆S

Guidance literature:: Multi-step reaction with 10 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 °C

2: 2,2,6,6-tetramethyl-piperidine; n-butyllithium; diethylaluminium chloride / hexane; toluene / 1.33 h / 0 °C

3: Grubbs catalyst first generation; p-benzoquinone / dichloromethane / 1 h / Reflux

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 20 °C / Inert atmosphere

5: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / Molecular sieve

6: fluorosilicic acid / water; acetonitrile / 18 h / 0 - 4 °C

7: sodium hydroxide / 1,4-dioxane; water / 6 h / 90 °C / Inert atmosphere

8: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 0.83 h / -78 - 20 °C

9: manganese(IV) oxide / chloroform / 20 °C

10: dmap / dichloromethane

With 2,2,6,6-tetramethyl-piperidine; Grubbs catalyst first generation; dmap; manganese(IV) oxide; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; fluorosilicic acid; diethylaluminium chloride; sodium hydride; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; p-benzoquinone; sodium hydroxide; In 1,4-dioxane; methanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; benzene;
DOI:10.1021/jo3008034