[Co(en)2(μ-O3POC6H5)]2Cl2*2H2O

Base Information

Chemical Name:[Co(en)2(μ-O3POC6H5)]2Cl2*2H2O
CAS No.:83023-97-6
Molecular Formula:C₂₀H₄₂Co₂N₈O₈P₂*2Cl*2H₂O
Molecular Weight:809.473
Hs Code.:

Synonyms:

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Chemical Property of [Co(en)2(μ-O3POC6H5)]2Cl2*2H2O

Chemical Property:

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Technology Process of [Co(en)2(μ-O3POC6H5)]2Cl2*2H2O

There total 1 articles about [Co(en)2(μ-O3POC6H5)]2Cl2*2H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cis-{CoCl₂en2}ClO₄

: 66924-56-9
disilver phenyl phosphate

: 83023-97-6
[Co(en)2(μ-O3POC6H5)]2Cl2*2H2O

Guidance literature:: With NaI; In dimethyl sulfoxide; byproducts: AgI; the complex was dissolved at 80°C, powdered Ag2O3POPh was added,mixt. was srirred for 70 min, after the mixt. was cooled to room temp.,mixt. was poured into ice-cold water; NaI was added and AdI then was removed, mixt. was chromd., soln. was evapd., then cooled at 0°C for 4 h, ppt. was washed with ice-cold LiCl soln., MeOH and Et2O, it was then dried; elem.anal.;
DOI:10.1021/ic00142a010

Reference yield:

: 83023-97-6
[Co(en)2(μ-O3POC6H5)]2Cl2*2H2O

: 2926-30-9
sodium triflate

: 83023-99-8
[Co(en)2(μ-O3POC6H5)]2(CF3SO3)2*2H2O

Guidance literature:: In water; the complex was dissolved in hot water and filtered, Na(CF3SO3) was added, the soln. was cooled to 4°C and standed overnight; ppt. was washed with ice-cold Na(CF3SO3) soln., MeOH and ether, it was then dried over P2O5 for 3 days; elem.anal.;
DOI:10.1021/ic00142a010

Reference yield:

: 83023-97-6
[Co(en)2(μ-O3POC6H5)]2Cl2*2H2O

: sodium perchlorate

: 83024-01-5
meso-[Co(en)2(μ-O3POC6H5)]2(ClO4)2*2H2O

: 83057-66-3
rac-[Co(en)2(μ-O3POC6H5)]2(ClO4)2*2H2O

Guidance literature:: In water; the complex was dissolved in hot water and filtered, NaClO4 was added and mixt. was stirred for 1 h; ppt. was washed with MeOH and ether, solid was then suspd. in water andchromd., isomers were sepd., ppt. were washed with ice-cold NaClO4, MeOH, etherand dried;elem.anal.;
DOI:10.1021/ic00142a010