bis(2,4,6-triphenylphenyl)germylene

Base Information

• Chemical Name: bis(2,4,6-triphenylphenyl)germylene
• CAS No.: 328396-59-4
• Molecular Formula: C₄₈H₃₄Ge
• Molecular Weight: 683.388
• Mol file: 328396-59-4.mol

Synonyms:

Chemical Property of bis(2,4,6-triphenylphenyl)germylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of bis(2,4,6-triphenylphenyl)germylene

There total 1 articles about bis(2,4,6-triphenylphenyl)germylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

germanium(II) chloride dioxane + 2,4,6-triphenylphenyllithium bis(diethyl ether) → bis(2,4,6-triphenylphenyl)germylene (328396-59-4)

Guidance literature:

In diethyl ether; stirred under N2 at -50°C for 2 h and for 6 h at room temp.; volatiles removed in vacuo, residue extd. with toluene and evpd.; elem. anal.;

DOI:10.1021/om000743t

Reference yield: 83.0%

trimethylamine-N-oxide (1184-78-7) + bis(2,4,6-triphenylphenyl)germylene (328396-59-4) → bis(2,4,6-triphenylphenyl)germanone (327179-03-3)

Guidance literature:

In tetrahydrofuran; stirred under N2 at room temp. for 24 h; volatiles removed in vacuo, residue washed with pentane, extd. with toluene and evpd.; elem. anal.;

DOI:10.1021/om000743t

Downstream raw materials:

bis(2,4,6-triphenylphenyl)germanone