2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2

Base Information

Chemical Name:2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2
CAS No.:1141819-53-5
Molecular Formula:C₇H₁₄BrNO₂
Molecular Weight:226.082
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Chemical Property of 2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2

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Technology Process of 2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2

There total 1 articles about 2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1141819-49-9
2-[(tert-butoxycarbonyl)amino]ethanol-2,2-d2

: 1141819-53-5
2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/chem.201002759

Reference yield:

: 1141819-53-5
2-[(tert-butoxycarbonyl)amino]ethyl bromide-2,2-d2

: C₁₃⁽¹³⁾CH₁₉⁽²⁾H₂N₃O₆S

Guidance literature:: Multi-step reaction with 3 steps

1: 18-crown-6 ether / acetonitrile / 9 h / 80 °C

2: platinum(IV) oxide; hydrogen / methanol / 22 h / 20 °C / 3420.23 Torr

3: triethylamine / dichloromethane / 8 h / 20 °C

With platinum(IV) oxide; 18-crown-6 ether; hydrogen; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/chem.201002759