5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N²-isobutyryl-2’,3’-O-isopropylidene-O⁶-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine

Base Information

• Chemical Name: 5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N²-isobutyryl-2’,3’-O-isopropylidene-O⁶-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine
• CAS No.: 1449295-02-6
• Molecular Formula: C₇₄H₈₇N₉O₁₅SSi
• Molecular Weight: 1402.71

Synonyms:

Chemical Property of 5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N²-isobutyryl-2’,3’-O-isopropylidene-O⁶-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine

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Technology Process of 5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N²-isobutyryl-2’,3’-O-isopropylidene-O⁶-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine

There total 1 articles about 5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N²-isobutyryl-2’,3’-O-isopropylidene-O⁶-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C40H39N3O7S + 5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N2-isobutyryl-2’,3’-O-isopropylidene-8-{[(methylsulfonyl)oxy]methyl}-O6-[2-(4-nitrophenyl)ethyl]guanosine (1449294-99-8) → 5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N2-isobutyryl-2’,3’-O-isopropylidene-O6-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine (1449295-02-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; for 6h;

DOI:10.1002/hlca.201300043

Reference yield:

5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N2-isobutyryl-2’,3’-O-isopropylidene-O6-[2-(4-nitrophenyl)ethyl]guanosine-8-methyl-(815’-S)-N4-benzoyl-2’,3’-O-isopropylidene-6-{[ (4-methoxyphenyl)diphenylmethoxy]methyl}-5’-thiocytidine (1449295-02-6) → C54H71N9O14SSi

Guidance literature:

With dichloro-acetic acid; chlorotriisopropylsilane; In dichloromethane; for 1h;

DOI:10.1002/hlca.201300043

upstream raw materials:

5’-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-N2-isobutyryl-2’,3’-O-isopropylidene-8-{[(methylsulfonyl)oxy]methyl}-O⁶-[2-(4-nitrophenyl)ethyl]guanosine

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