Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

Base Information

Chemical Name:Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)
CAS No.:138695-26-8
Molecular Formula:C₄₆H₃₇O₄P₂Re
Molecular Weight:901.952
Hs Code.:

Re(CO)3(P(C<sub>6</sub>H<sub>5</sub>)3)2(OC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)

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Chemical Property of Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

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Technology Process of Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

There total 1 articles about Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 106-44-5
p-cresol

: Re(CO)3(P(C₆H₅)3)2(CH₃)

: 138695-26-8
Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

Guidance literature:: In benzene; byproducts: CH4; at 45°C;

Reference yield: 77.0%

: 138695-26-8
Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

: 13246-32-7
ortho-phenylenebis(dimethylarsine)

: 144812-17-9
Re(CO)3(OC₆H₄CH₃)(C₆H₄(As(CH₃)2)2)

Guidance literature:: In benzene; byproducts: P(C6H5)3; addn. of o-phenylenebis(dimethylarsine) to Re-compound in C6H6; heating in a bomb at 46°C for 12 h; inert atm.;; removal of benzene under vac.; washing with hexane; analytically pure;;
DOI:10.1021/om00027a031

Reference yield: 61.0%

: 138695-26-8
Re(CO)3(P(C₆H₅)3)2(OC₆H₄CH₃)

: 594-09-2
trimethylphosphane

: 144812-13-5
(CO)3(P(CH₃)3)2Re(OC₆H₄CH₃)

Guidance literature:: In benzene; byproducts: P(C6H5)3; charging a bomb with Re-compound in C6H6; condensation of P(CH3)3 into the bomb at -196°C; heating to 45°C overnight; inert atm.;; concn.; pptn. by addn. of hexanes; filtration; washing with hexane; dissolving in toluene; layering with pentane; cooling to -40°C overnight; crystallization; filtration; washing with hexane; drying in high vac. for 12 h; elem. anal.;;
DOI:10.1021/om00027a031