Cu(3-phenylthioacetylacetonate)2

Base Information

• Chemical Name: Cu(3-phenylthioacetylacetonate)2
• CAS No.: 76401-10-0
• Molecular Formula: C₂₂H₂₂CuO₄S₂
• Molecular Weight: 478.092
• Mol file: 76401-10-0.mol

Synonyms:

Chemical Property of Cu(3-phenylthioacetylacetonate)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Cu(3-phenylthioacetylacetonate)2

There total 1 articles about Cu(3-phenylthioacetylacetonate)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

3-(phenylthio)pentane-2,4-dione (22805-23-8) + copper dichloride → Cu(3-phenylthioacetylacetonate)2 (76401-10-0)

Guidance literature:

With sodium acetate; In ethanol; water; soln. of 0.0033 mol of sodium acetate in 5 ml of H2O added dropwise withstirring to combined solns. of 0.001 mol of metal chloride in H2O and 0 .0033 mol of diketone in 5 ml of alc.; mixt. heated until oil pptd.; mixt. diluted (H2O); extd. (CHCl3); solvent removed; residue recrystd. (hexane, alc.); elem. anal.;

DOI:10.1134/S1070363207110035

Reference yield: 81.0%

Cu(3-phenylthioacetylacetonate)2 (76401-10-0) → 3,5-dimethyl-4-phenylsulfanyl-1H-pyrazole (127788-13-0)

Guidance literature:

With hydrazine hydrate; for 2h; regioselective reaction; Reflux;

DOI:10.1134/S1070363211040244

upstream raw materials:

3-(phenylthio)pentane-2,4-dione

Downstream raw materials:

3,5-dimethyl-4-phenylsulfanyl-1H-pyrazole