α-Oxetanocin

Base Information

Chemical Name:α-Oxetanocin
CAS No.:120293-59-6
Molecular Formula:C₁₀H₁₃N₅O₃
Molecular Weight:251.245
Hs Code.:

Synonyms:

Suppliers and Price of α-Oxetanocin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-Oxetanocin

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of α-Oxetanocin

There total 19 articles about α-Oxetanocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 120293-57-4
N,N-dibenzoylepioxetanocin dibenzoate

: 120293-59-6,132077-74-8
α-Oxetanocin

Guidance literature:: With sodium methylate; In methanol; Ambient temperature;
DOI:10.1016/S0040-4039(00)80596-1

Reference yield:

: 69832-48-0
((3aR,5S,6R,6aR)-tetrahydro-2,2-dimethyl-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)furo[2,3-d][1,3]dioxol-6-yl)methanol

: 120293-59-6,132077-74-8
α-Oxetanocin

Guidance literature:: Multi-step reaction with 14 steps

1: AcOH / H₂O

2: NaIO₄ / ethanol; H₂O

3: NaBH₄ / ethanol

4: NaH / dimethylformamide

5: aq. TFA

6: Br₂, barium benzoate / H₂O; dioxane

7: pyridine / CH₂Cl₂ / -30 °C

8: 56 percent / K₂CO₃

9: hydrolyse

10: oxalyl chloride

12: decarboxylative chlorination

13: K₂CO₃

14: 1) NaOH, 2) H₂ / palladium hydroxide / 1) MeOH, 2) cyclohexene

With pyridine; sodium hydroxide; sodium tetrahydroborate; sodium periodate; oxalyl dichloride; hydrogen; bromine; sodium hydride; potassium carbonate; acetic acid; barium benzoate; trifluoroacetic acid; palladium dihydroxide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)97210-1

Reference yield:

: 69827-89-0
((3aR,5S,6R,6aR)-5-Hydroxymethyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl)-methanol

: 120293-59-6,132077-74-8
α-Oxetanocin

Guidance literature:: Multi-step reaction with 11 steps

1: NaH / dimethylformamide

2: aq. TFA

3: Br₂, barium benzoate / H₂O; dioxane

4: pyridine / CH₂Cl₂ / -30 °C

5: 56 percent / K₂CO₃

6: hydrolyse

7: oxalyl chloride

9: decarboxylative chlorination

10: K₂CO₃

11: 1) NaOH, 2) H₂ / palladium hydroxide / 1) MeOH, 2) cyclohexene

With pyridine; sodium hydroxide; oxalyl dichloride; hydrogen; bromine; sodium hydride; potassium carbonate; barium benzoate; trifluoroacetic acid; palladium dihydroxide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)97210-1